2
|
5.63 s |
5.62 s |
5.56 s |
5.99 s |
5.93 s |
5.62 s |
4
|
- |
- |
2.89 q J 4,15 = 7.2 |
3.56 q J4,15 = 7.2 |
3.45 q J 4,15 = 7.2 |
- |
5
|
6.04-6.03 m |
6.03-6.00 m |
2.99 brs |
3.97 brs |
3.88 brs |
6.03-6.01 m |
6
|
5.02-4.98 m |
5.02-4.97 m |
4.26 d J6,7 = 6.5 |
4.74 a |
4.73 d J6,7 = 7.9 |
4.90-4.86 m |
7
|
2.82 dd J6,7 = 7.1; J7,8 = 4.2 |
2.87 dd J6,7 = 7.3; J7,8 = 4.2 |
2.95 dd J6,7 = 6.5; J7,8 = 4.9 |
3.09 dd J6,7 = 7.8; J7,8 = 4.2 |
3.04 dd J6,7 = 7.8; J7,8 = 4.3 |
2.84 dd J6,7 = 7.2; J7,8 = 4.4 |
8
|
4.09 ddd J7,8 = 4.2; J8,9a = 2.5; J8,9b = 12.0 |
4.07 ddd J7,8 = 4.2; J8,9a = 2.6; J8,9b = 11.9 |
3.91 ddd J7,8 = 4.9; J8,9a = 2.3; J8,9b = 11.9 |
3.92 m |
3.96 ddd J7,8 = 4.3; J8,9a = 2.8; J8,9b = 113 |
3.85 ddd J7,8 = 4.4; J8,9a = 2.4; J8,9b = 12.0 |
9a
|
2.48 dd J8,9a = 2.5; J9a,9b = 13.5 |
2.39 dd J8,9a = 2.6; J9a,9b = 13.6 |
2.39 dd J8,9a = 2.3; J9a,9b = 13.5 |
2.32 dd J8,9a = 2.3; J9a,9b = 13.6 |
2.27 dd J8,9a = 2.8; J9a,9b = 13.8 |
2.41 dd J8,9a = 2.4; J9a,9b = 13.6 |
9b
|
2.00 dd J8,9b = 12.0; J9a,9b = 13.5 |
1.94 dd J8,9b = 11.9; J9a,9b = 13.6 |
1.90 dd J8,9b = 11.9; J9a,9b = 13.5 |
2.39 J8,9b = 11.5; J9a,9b = 13.6 |
2.34 dd J8,9b = 11.3; J9a,9b = 13.8 |
2.06 dd J8,9b = 12.0; J9a,9b = 13.6 |
13
|
1.18 s |
1.33 s |
1.38 s |
1.39 s |
1.21 s |
1.16 s |
14
|
1.45 s |
1.48 s |
1.43 s |
1.50 s |
1.45 s |
1.50 s |
15
|
2.05 t J5.15 =6,15= 1.9 |
2.05 t J5,15 =6,15= 2.0 |
1.37 d J4,15 = 7.2 |
1.52 d J4,15 = 7.2 |
1.48 d J4,15 = 7.2 |
2.06 dd J5,15 = 2.0; J6,15 = 1.6 |
2′a
|
5.31 brs |
3.11 d J2′a,2′b = 5.5 |
3.12 d J2′a,2′b = 5.5 |
4.04 d J2′a,2′b = 11.9 |
5.22 brs |
5.28 d J2′a,2′b = 1.2 |
2′b
|
5.07 t J2′a,2′b = 1.6 |
2.70 d J2′a,2′b = 5.5 |
2.71 d J2′a,2′b = 5.5 |
3.75 d J2′a,2′b = 11.9 |
5.13 t J2′a,2′b = 1.4 |
5.13 brs |
3′
|
1.91 s |
1.55 s |
1.57 s |
1.50 s |
1.77 s |
1.79 s |
4′a
|
- |
- |
2.8 dt J4′a,4′b = 11.2; J4′a,5′ = 7.0 |
3.28 td J4′a,4′b = 11.2; J4′a,5′ = 5.8; |
3.18 dt J4′a,4′b = 10.5; J4′a,5′ = 5.7 |
3.36 dq J4′a,4′b = 9.2; J4′a,5′ =7.2 |
4′b
|
- |
- |
2.53 dt J4′a,4′b = 11.2; J4′b,5′ = 6.9; |
3.17 td J4′a,4′b = 11.2; J4′b,5′ =5.8 |
3.09 dt J4′a,4′b = 10.5; J4′b,5′ =5.7 |
3.20 m |
5′
|
- |
- |
1.50 m |
1.80 m |
1.75 m |
1.07 t J4′a,5′ =,4′b,5′ = 7.2 |
6′
|
- |
- |
0.93 t J5′,6′ = 7.3 |
0.99 t J5′,6′ = 7.4 |
0.94 t J5′,6′ = 7.3 |
- |
OH
|
3.79 s |
3.69 s |
|
|
|
|