Cromatografia de extratos de <i>Solanum habrochaites</i> com o primeiro registro de etil docosanoato, hexadecanoato e octadecanoato nesta planta e em Solanaceae

Santos, C. A. M.; Teixeira, D. L.; Salgado-Neto, G.; Wilcken, C. F.; Lemes, P. G.; Tavares, W. S.; Sabattini, J. A.; Zanuncio, J. C.

C. A. M. Santos

Universidade Federal de Viçosa – UFV, Instituto de Biotecnologia Aplicada à Agricultura, Departamento de Entomologia, Viçosa, MG, Brasil

https://orcid.org/0000-0002-4270-1003

D. L. Teixeira ^**e-mail: david.l.teixeira@ufv.br

Universidade Federal de Viçosa – UFV, Instituto de Biotecnologia Aplicada à Agricultura, Departamento de Entomologia, Viçosa, MG, Brasil

https://orcid.org/0000-0002-3793-0792

G. Salgado-Neto

Universidade Federal de Santa Maria – UFSM, Departamento de Defesa Fitossanitária, Programa de Pós-graduação em Agronomia, Santa Maria, RS, Brasil

https://orcid.org/0000-0002-0431-9700

C. F. Wilcken

Universidade Estadual Paulista “Júlio de Mesquita Filho” – UNESP, Faculdade de Ciências Agronômicas, Departamento de Proteção Vegetal, Botucatu, SP, Brasil

https://orcid.org/0000-0001-9875-4158

P. G. Lemes

Universidade Federal de Minas Gerais – UFMG, Instituto de Ciências Agrárias, Laboratório de Entomologia Aplicada a Área Florestal, Montes Claros, MG, Brasil

https://orcid.org/0000-0002-1364-0424

W. S. Tavares

PT. ITCI Hutani Manunggal - IHM, Balikpapan, East Kalimantan, Indonesia

https://orcid.org/0000-0002-8394-6808

J. A. Sabattini

Universidad Nacional de Entre Ríos, Fuacultad de Ciencias Agropecuarias, Consejo Nacional de Investigaciones Científicas y Técnicas, Departmento de Ecología, Oro Verde, Argentina

https://orcid.org/0000-0001-6449-3391

J. C. Zanuncio

Universidade Federal de Viçosa – UFV, Instituto de Biotecnologia Aplicada à Agricultura, Departamento de Entomologia, Viçosa, MG, Brasil

https://orcid.org/0000-0003-2026-281X

*e-mail: david.l.teixeira@ufv.br

Factions Comp.	Compound	Area	RI	RI*	Ref.
1	Hexadecanoic acid	2.23	1975	1973	1
2	Docosane	0.99	2205	2200	2
3	Tricosane	2.70	2305	2302	1
Fraction F1 4	Pentacosane	5.31	2506	2500	2
5	Heptacosane	11.54	2712	2700	3
6	Octacosane	1.58	2806	2800	4
7	Squalene	2.97	2855	2847	2
8	Ethyl hexadecanoate	8.91	2010	2013	5
9	Ethyl octadecanoate	2.71	2204	2207	6
Fraction 2 10	Ethyl docosanoate	0.56	2601	2596	7
11	Tridecan-2-one	38.02	1512	1512	8
12	Pentadecan-2-one	4.46	1705	1705	9
Fraction 5 13	6,10,14-Trimethylpentadecan-2-one	20.05	1856	1846	10
14	9,12,15-Ocadecatrienal	1.18	1973	1979	11

RI= Retention Index.*reported in literature. 1- Hosseinihashemi et al. (2013)HOSSEINIHASHEMI, S.K., SAFDARI, V. and KANANI, S., 2013. Comparative chemical composition of n-hexane and ethanol extractives from the heartwood of black locust. Asian Journal of Chemistry, vol. 25, no. 2, pp. 929-933. http://doi.org/10.14233/ajchem.2013.13159.
http://doi.org/10.14233/ajchem.2013.1315... , 2- Samejo et al. (2013)SAMEJO, M.Q., MEMON, S., BHANGER, M.I. and KHAN, K.M., 2013. Comparison of chemical composition of Aerva javanica seed essential oils obtained by different extraction methods. Pakistan Journal of Pharmaceutical Sciences, vol. 26, no. 4, pp. 757-760. PMid:23811454., 3- Silva et al. (2013)SILVA, E.B.P., SOARES, M.G., MARIANE, B., VALLIM, M.A., PASCON, R.C., SARTORELLI, P. and LAGO, J.H.G., 2013. The seasonal variation of the chemical composition of essential oils from Porcelia macrocarpa R.E. Fries (Annonaceae) and their antimicrobial activity. Molecules , vol. 18, no. 11, pp. 13574-13587. http://doi.org/10.3390/molecules181113574. PMid:24189296.
http://doi.org/10.3390/molecules18111357... , 4- Naquvi et al. (2014)NAQUVI, K.J., ANSARI, S.H., ALI, M. and NAJMI, A.K., 2014. Volatile oil composition of Rosa damascena Mill. (Rosaceae). Journal of Pharmacognosy and Phytochemistry, vol. 2, no. 5, pp. 177-181., 5- Selli et al. (2006)SELLI, S., RANNOU, C., PROST, C., ROBIN, J. and SEROT, T., 2006. Characterization of aroma-active compounds in rainbow trout (Oncorhynchus mykiss) eliciting an off-odor. Journal of Agricultural and Food Chemistry, vol. 54, no. 25, pp. 9496-9502. http://doi.org/10.1021/jf0619582. PMid:17147438.
http://doi.org/10.1021/jf0619582... , 6- Ansorena et al. (2000)ANSORENA, D., ASTIASARÁN, I. and BELLO, J., 2000. Influence of the simultaneous addition of the protease flavourzyme and the lipase novozyme 677BG on dry fermented sausage compounds extracted by SDE and analyzed by GC-MS. Journal of Agricultural and Food Chemistry, vol. 48, no. 6, pp. 2395-2400. http://doi.org/10.1021/jf990931y. PMid:10888557.
http://doi.org/10.1021/jf990931y... , 7- Heinrich et al. (2002)HEINRICH, G., PFEIFHOFER, H.W., STABENTHEINER, E. and SAWIDIS, T., 2002. Glandular hairs of Sigesbeckia jorullensis Kunth (Asteraceae): morphology, histochemistry and composition of essential oil. Annals of Botany, vol. 89, no. 4, pp. 459-469. http://doi.org/10.1093/aob/mcf062. PMid:12096807.
http://doi.org/10.1093/aob/mcf062... , 8- Owens et al. (1997)OWENS, J.D., ALLAGHENY, N., KIPPING, G. and AMES, J.M., 1997. Formation of volatile compounds during Bacillus subtilis fermentation of soya beans. Journal of the Science of Food and Agriculture, vol. 74, no. 1, pp. 132-140. http://doi.org/10.1002/(SICI)1097-0010(199705)74:1<132::AID-JSFA779>3.0.CO;2-8.
http://doi.org/10.1002/(SICI)1097-0010(1... , 9- Souza et al. (2009)SOUZA, P.P., CARDEAL, Z.D.E.L., AUGUSTI, R., MORRISON, P. and MARRIOTT, P.J., 2009. Determination of volatile compounds in Brazilian distilled cachaca by using comprehensive two-dimensional gas chromatography and effects of production pathways. Journal of Chromatography. A, vol. 1216, no. 14, pp. 2881-2890. http://doi.org/10.1016/j.chroma.2008.10.061. PMid:19004451.
http://doi.org/10.1016/j.chroma.2008.10.... , 10- Shi-Dong et al. (2014)SHI-DONG, L., YUAN-SHUANG, W., JIANG-SHENG, Z., MING, L. and QING-XIONG, M., 2014. Analysis of aroma components of dark teas from five different production regions by fully automatic headspace solid-phase microextraction coupled with gas chromatography-mass spectrometry. Journal of Chemical and Pharmaceutical Research, vol. 6, no. 1, pp. 246-253., 11- Yang et al. (2012)YANG, Z., ZHU, S. and YU, Z., 2012. Comparison of terpene components from flowers of Artemisia annua. Bangladesh Journal of Pharmacology, vol. 7, no. 2, pp. 114-119. http://doi.org/10.3329/bjp.v7i2.10815.
http://doi.org/10.3329/bjp.v7i2.10815... .

[1] *e-mail: david.l.teixeira@ufv.br

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Cromatografia de extratos de Solanum habrochaites com o primeiro registro de etil docosanoato, hexadecanoato e octadecanoato nesta planta e em Solanaceae

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