Establishment of a novel pork kidney lavage method and detection of heavy metals and antibiotics

LIANG, Zhijuan; TAN, Hailin; LI, Dan; LIANG, Ye; WANG, Liping; CHEN, Yuanbin; NIU, Haitao

doi:10.1590/fst.09622

Acessibilidade / Reportar erro

Brasil

Food Science and Technology

Español English

Brasil

Español English

sumário « anterior atual seguinte »

Sumário

Original Article • Food Sci. Technol 42 • 2022 • https://doi.org/10.1590/fst.09622 copy

Establishment of a novel pork kidney lavage method and detection of heavy metals and antibiotics

Authorship SCIMAGO INSTITUTIONS RANKINGS

Abstract

The effectiveness and feasibility of a pork kidney lavage method to remove heavy metals and antibiotics from fresh pork kidney were investigated. This work provides a basis for the research and development of contaminant-free pork kidney foods. A comparative study was performed on pork kidneys with traditional treatment versus lavage treatment. The contents of Cu, Pb and Hg, 18 sulfonamides, 15 quinolones, ampicillin and cefalexin were detected by FAAS, GF-AAS, AFS and LC-MS/MS. The detection results of heavy metals and antibiotics showed that the content of Cu in pork kidney after lavage was significantly reduced, and antibiotics such as sulfachlorpyridazine and enrofloxacin were not detected. Therefore, lavage is an effective method to remove toxins from fresh pork kidney and can remove heavy metals and antibiotics to the maximum extent, providing a basic guarantee for the production of contaminant-free pork kidney foods.

Keywords:
pork kidney; lavage; heavy metals; antibiotics; contaminant-free

Test item	Unit	Test basis	Value (Unlavage)	Value (Lavage)
Pb	mg/kg	GB5009.12-2017	Non-Detected (< 0.04)	Non-Detected (< 0.04)
Cu	µg/kg	GB5009.13-2017	5.8	4.4
Hg	µg/kg	GB5009.17-2014	Non-Detected (< 0.01)	Non-Detected (< 0.01)

Test item	Unit	Test basis	Value (Unlavage)	Value (Lavage)
Sulphaguanidine	µg/kg	GB/T 21316-2007	Non-Detected (< 50)	Non-Detected (< 50)
Sulfaphenazole	µg/kg	GB/T 21316-2007	Non-Detected (< 50)	Non-Detected (< 50)
Sulfabenzamide	µg/kg	GB/T 21316-2007	Non-Detected (< 50)	Non-Detected (< 50)
Sulfapyridine	µg/kg	GB/T 21316-2007	Non-Detected (< 50)	Non-Detected (< 50)
Sulfacetamide	µg/kg	GB/T 21316-2007	Non-Detected (< 50)	Non-Detected (< 50)
Sulfadimethoxine	µg/kg	GB/T 21316-2007	Non-Detected (< 50)	Non-Detected (< 50)
Sulfametoxydiazine	µg/kg	GB/T 21316-2007	Non-Detected (< 50)	Non-Detected (< 50)
Sulfadoxine	µg/kg	GB/T 21316-2007	Non-Detected (< 50)	Non-Detected (< 50)
Sulfadimidine	µg/kg	GB/T 21316-2007	Non-Detected (< 50)	Non-Detected (< 50)
Sulfamethoxazole	µg/kg	GB/T 21316-2007	Non-Detected (< 50)	Non-Detected (< 50)
Sulfamethazine	µg/kg	GB/T 21316-2007	Non-Detected (< 50)	Non-Detected (< 50)
Sulfamethoxypyridazine	µg/kg	GB/T 21316-2007	Non-Detected (< 50)	Non-Detected (< 50)
Sulfamonomethoxine	µg/kg	GB/T 21316-2007	Non-Detected (< 50)	Non-Detected (< 50)
Sulfaquinoxaline	µg/kg	GB/T 21316-2007	Non-Detected (< 50)	Non-Detected (< 50)
Sulfachlorpyridazine	µg/kg	GB/T 21316-2007	57.8	Non-Detected (< 50)
Sulfadiazine	µg/kg	GB/T 21316-2007	Non-Detected (< 50)	Non-Detected (< 50)
Sulfathiazole	µg/kg	GB/T 21316-2007	Non-Detected (< 50)	Non-Detected (< 50)
Sulfanitran	µg/kg	GB/T 21316-2007	Non-Detected (< 50)	Non-Detected (< 50)

Test item	Unit	Test basis	Value (Unlavage)	Value (Lavage)
Orbifloxacin	µg/kg	SN/T 1751.2-2007	Non-Detected (< 10.0)	Non-Detected (< 10.0)
Marbofloxacin	µg/kg	SN/T 1751.2-2007	Non-Detected (< 10.0)	Non-Detected (< 10.0)
Difloxacin	µg/kg	SN/T 1751.2-2007	Non-Detected (< 10.0)	Non-Detected (< 10.0)
Sparfloxacin	µg/kg	SN/T 1751.2-2007	Non-Detected (< 10.0)	Non-Detected (< 10.0)
Fleroxacin	µg/kg	GB/T 20366-2006	Non-Detected (< 1.0)	Non-Detected (< 1.0)
Danofloxacin	µg/kg	GB/T 21312-2007	Non-Detected (< 3.0)	Non-Detected (< 3.0)
Enrofloxacin	µg/kg	GB/T 21312-2007	11.8	Non-Detected (< 3.0)
Ciprofloxacin	µg/kg	GB/T 21312-2007	Non-Detected (< 8)	Non-Detected (< 8)
Lomefloxacin	µg/kg	GB/T 21312-2007	Non-Detected (< 3.0)	Non-Detected (< 3.0)
Norfloxacin	µg/kg	GB/T 21312-2007	Non-Detected (< 6)	Non-Detected (< 6)
Pefloxacin	µg/kg	GB/T 21312-2007	Non-Detected (< 6)	Non-Detected (< 6)
Sarafloxacin	µg/kg	GB/T 21312-2007	Non-Detected (< 6)	Non-Detected (< 6)
Enoxacin	µg/kg	GB/T 21312-2007	Non-Detected (< 10)	Non-Detected (< 10)
Ofloxacin	µg/kg	GB/T 21312-2007	Non-Detected (< 3.0)	Non-Detected (< 3.0)
Cinoxacin	µg/kg	GB/T 21312-2007	Non-Detected (< 6)	Non-Detected (< 6)

Test item	Unit	Test basis	Value (Unlavage)	Value (Lavage)
Ampicillin	µg/kg	GB/T 21315-2007	Non-Detected (< 5)	Non-Detected (< 5)
Cefalexin	µg/kg	SN/T 1988-2007	Non-Detected (< 2)	Non-Detected (< 2)

Sociedade Brasileira de Ciência e Tecnologia de Alimentos Av. Brasil, 2880, Caixa Postal 271, 13001-970 Campinas SP - Brazil, Tel.: +55 19 3241.5793, Tel./Fax.: +55 19 3241.0527 - Campinas - SP - Brazil
E-mail: revista@sbcta.org.br

Acompanhe os números deste periódico no seu leitor de RSS

[1] *Corresponding author: niuht0532@126.com