DMSPE5656 Babaee, S.; Daneshfar, A.; J. Sep. Sci. 2016, 39, 2508.
|
2-NP, Ph, p-cresol, carvacrol, 2-tert-butylphenol, mequinol, 4-CP, resorcinol |
water |
sorbent: 20 mg PANI/SiO2/Ni NPs; sample volume: 5 mL; adsorption: 30 s sonication + 5 min vortex; eluent: 40 µL ACN; desorption: 11.5 min sonication |
GC-FID |
linear range: 0.02-100 mg L-1 LOD: 10-23 µg L-1 LOQ: 33-77 µg L-1 R: 96-105% RSD: < 4% |
MSPE3939 Zhou, Q.; Yuan, Y.; Wu, Y.; Liu, Y.; J. Sep. Sci. 2017, 40, 4032.
|
bisphenol A, tetrabromobisphenol A, 4-nonylphenol |
water |
sorbent: 60 mg PANI@SiO2@Fe; sample volume: 60 mL; adsorption: 60 min shaking on a temperature-controlled water-bath; eluent: 7.5 mL MeOH (dried with N2 at 40 ºC and redissolved with 200 µL MeOH) |
HPLC-UV |
linear range: 0.05-300 µg L-1 LOD: 0.009-0.073 µg L-1 R: 92.9-98.9% RSD: < 3.73% |
SB-µ-SPE77 Tanimu, A.; Jillani, S. M. S.; Alluhaidan, A. A.; Ganiyu, S. A.; Alhooshani, K.; Talanta 2019, 194, 377.
|
24DCP, 23DCP, 26DCP, 246TCP, 26DTB4MP, 4tOP, 2B4CP |
wastewater |
sorbent: 20 mg 4-phenyl-1,2,3-triazole functionalized SBA-15 sealed inside a PP bag; adsorption: 15 min stirring; eluent: 300 µL ethyl acetate; desorption: 20 min sonication |
GC-MS |
linear range: 1-600 µg L-1 LOD: 0.23-0.37 µg L-1 R: 88.5-99.2% RSD: 2.3-7.5% |
Online MMD-SPE33 Ghani, M.; Picó, M. F. F.; Salehinia, S.; Cabello, C. P.; Maya, F.; Berlier, G.; Saraji, M.; Cerdà, V.; Palomino, G. T.; J. Chromatogr. A 2017, 1488, 1.
|
4NP, 2CP, 24DNP, 2NP, 24DMP, 4C3MP, 24DCP |
groundwater |
sorbent: polyvinylidene fluoride matrix disks containing entrapped UiO-66-NH2 MOFs; sample volume: 1.5 mL; eluent: 0.3 mL acetone; desorption flow rate: 0.5 mL min-1
|
HPLC-DAD |
linear range: 0.5-500 µg L-1 LOD: 0.1-0.2 µg L-1 R: 90-98% RSD: 3.9-5.7% (intraday), 4.7-5.7% (inter-day) |
In-syringe extraction55 Tang, S.; Sun, J.; Xia, D.; Zang, B.; Gao, Y.; Chen, C.; Shen, W.; Lee, H. K.; Talanta 2019, 195, 165.
|
Ph, 4NP, 2NP, 3MP, 4C3MP, 24DCP, 2M46DNP, 246TCP, PCP |
river water |
sorbent: 5 mg graphene aerosols filled in 2-mL syringe; sample volume: 40 mL; adsorption: 20 min; eluent: 200 µL ACN |
HPLC-UV |
linear range: 0.05-20 µg L-1 LOD: 0.016-0.075 µg L-1 LOQ: 0.053-0.250 µg L-1 R: 96.3-102.4% RSD: < 5.4% |
VA-D-µ-SPE44 Boontongto, T.; Siriwong, K.; Burakham, R.; Chromatographia 2018, 81, 735.
|
Ph, 4NP, 24DNP, 2NP, 4C3MP, 24DCP, 2M46DNP, 246TCP |
water |
sorbent: 30 mg NH2-MIL-53(Al) MOF; sample volume: 10 mL; adsorption: 10 s vortex; eluent: 1.5 mL ACN-HOAc (9.5:0.5 v/v); desorption: 10 s vortex |
HPLC-DAD |
linear range: 0.0015-10 mg L-1 LOD: 0.4-13.3 µg L-1 LOQ: 1.3-51.9 µg L-1 R: 72.3-111.4% RSD: < 10.4% |
MSPE (this study) |
Ph, 4NP, 2CP, 24DNP, 24DMP, 4C3MP, 24DCP, 246TCP |
water |
sorbent: 70 mg Fe@SiO2@PANI; sample volume: 10 mL; adsorption: 2 min vortex; eluent: 0.5 mL ACN; desorption: 30 s vortex |
HPLC-DAD |
linear range: 0.012-10.000 µg mL-1 LOD: 0.001-0.030 µg mL-1 LOQ: 0.012-0.090 µg mL-1 R: 83.4-118.5% RSD: < 11% |