Urine |
7-AF |
LC-ES-MS/MS |
0.025 |
DLLME |
Reproducibility, linearity and limit of detection. |
1212 Melwanki, M. B.; Chen, W. S.; Bai, H. Y.; Lin, T.-Y.; Fuh, M.-R.; Talanta 2009, 78, 618. [Crossref]
|
Urine |
AZ, DZ, OZ |
HPLC-UV |
0.3- 0.7 |
DLLME |
Linearity and limit of detection. |
1616 Vardini, M.T.; Mashayekhi, H. A.; Saber-Tehrani, M.; J. Liq. Chromatogr. Relat. Technol. 2012, 35, 988. [Crossref]
|
Plasma |
AZ, BZ, CZ, DZ, LZ, LM and TT |
UPLC-PDA |
1.7 - 10.6 |
UA-DLME |
Linearity (7 points in triplicate), selectivity (without description), limit of detection, limit of quantification, intra and inter-precision (2 concentrations), accuracy and recovery |
1313 Fernández, P.; González, C.; Pena, M. T.; Carro, A. M.; Lorenzo, R. A.; Anal. Chim. Acta 2013, 767, 88. [Crossref]
|
Water, urine, plasma, and pills |
CD |
HPLC-UV |
0.5 |
DLLME |
Limit of detection, limit of quantification, linearity (7 points in triplicate), accuracy (2 concentrations) |
3939 Khodadoust, S.; Ghaedi, M.; J. Sep. Sci. 2013, 36, 1734. [Crossref]
|
Ultrapure water, tap water, fruit juice, urine |
DZ, MZ and AZ |
GC-FID |
0.1- 0.2 |
SPE-DLLME |
Linearity (triplicate for each point), limit of detection, limit of quantification. |
4040 Ghobadi, M.; Yamini, Y.; Ebrahimpour, B.; J. Sep. Sci. 2014, 37, 287. [Crossref]
|
Whole Blood |
7-AC, 7-AF, 7-AN, α-HA, α-HE, AZ, BZ, CD, CB, CZ, DL, DF, DZ, EZ, FN, FB, HT, LZ, LM, MZ, NT, OZ, TZ and TO |
UHPLC-MS/MS |
2.0 |
UA-DLLME |
Limit of detection, limit of quantification, specificity, linearity, accuracy (5 replicates for 3 points), intra and inter-day precision (5 replicates for 3 points for 3 three days), recovery and matrix effect. |
3535 Fisichella, M.; Odoardi, S.; Strano-Rossi, S.; Microchem. J. 2015, 123, 33. [Crossref]
|
Serum |
NT and MZ |
HPLC-MWD |
0.017 and 0.086 |
UA-SEME-SFOD-DLLME |
Linearity (10 levels in triplicate), limit of detection, limit of quantification, recovery, intra and inter-day precision |
4141 Goudarzi, N.; Farsimadan, S.; Chamjangali, M. A.; Bagherian, G. A.; J. Sep. Sci. 2015, 38, 1673. [Crossref]
|
Urine |
CD, EZ, TZ, MZ, CZ, LZ, LM and ME |
CE-DAD |
50- 100 |
DLLME-FASS |
Linearity, limit of detection, limit of quantification, intra and inter-precision, accuracy, selectivity, recovery. |
1717 Oledzka, I.; Kulińska, Z.; Prahl, A.; Baczek, T.; J. Anal. Toxicol. 2015, 39, 436. [Crossref]
|
Urine, plasma |
OZ, AZ and DZ |
HPLC-UV |
0.4- 0.7 |
SPE-DLLME |
Linearity, limit of detection, limit of quantification, intra-day precision (2 levels in 5 replicates). |
77 Mashayekhi, H. A.; Khalilian, F.; J. Chromatogr. Sci. 2016, 54, 1068. [Crossref]
|
Pills, plasma and urine |
CP, DZ, SR |
HPLC-DAD |
2.7 |
UA-DLLME-SFOD |
Linearity, limit of detection, limit of quantification, intra-day precision (6 replicates for 3 leves). |
4242 Farsimadan, S.; Goudarzi, N.; Chamjangali, M. A.; Bagherian, G.; Microchem. J. 2016, 128, 47. [Crossref]
|
Plasma, urine and water |
AZ, DZ, FR and MZ |
GC-µECD |
0.005-0.01 |
BE-DLLME |
Linearity, enrichment factor, limit of detection and quantification, intra and inter-precision, selectivity and matrix effect. |
4343 Ghambarian, M.; Tajabadi, F.; Yaminib, Y.; Esrafilic, A. RSC Adv. 2016, 6, 114198. [Crossref]
|
Whole blood |
7-AF, AZ, BZ, CB, CZ, CT, DZ, EZ, LE, EI, FR, LM, MZ, OZ, PZ, TZ, TO, ZP and ZC |
LC-ESI-MS/MS |
0.003 - 4.74 |
IL-DLLME |
Selectivity, linearity with heteroscedasticity study, accuracy, intra and inter-precision (5 days), limit of quantification, limit of detection, recovery, accuracy, matrix effect and stability. |
88 De Boeck, M.; Missotten, S.; Dehaen, W.; Tygat, J.; Cuypers, E.; Forensic Sci. Int. 2017, 274, 44. [Crossref]
|
Urine |
FE, DC, FB and EI |
GC-QQQ-MS |
1 - 3 |
UA-LDS-DLLME |
Selectivity, linearity, accuracy, intra and inter-precision, limit of quantification, limit of detection, recovery. |
1818 Meng, L.; Zhu, B.; Zheng, K.; Fu, S.; J. Chromatogr. B: Anal. Technol. Biomed. Life Sci. 2017, 1053, 9. [Crossref]
|
Whole blood |
7-AF, AZ, BZ, CB, CZ, CT, DZ, EZ, LE, EI, FR, LM, MZ, OZ, PZ, TZ and TO |
LC-ESI-MS/MS |
0.003 - 4.74 |
IL-DLLME |
It was based Boeck and co-authors method88 De Boeck, M.; Missotten, S.; Dehaen, W.; Tygat, J.; Cuypers, E.; Forensic Sci. Int. 2017, 274, 44. [Crossref]. |
3636 De Boeck, M.; Dehaen, W.; Tytgat, J.; Cuypers, E.; J. Forensic Sci. 2018, 63, 1875. [Crossref]
|
Citrated plasma |
AZ, CZ, DZ and NZ |
HPLC-DAD |
40-50 |
UA-DLLME |
Limit of detection, limit of quantification, selectivity, specificity, linearity, intra and inter-day precision, accuracy, recovery, robustness, memory effect and dilution integrity. |
Proposed method |