ONE STRAIN-MANY COMPOUNDS (OSMAC) METHOD FOR PRODUCTION OF PHENOLIC COMPOUNDS USING <i>Camarops sp.</i>, AN ENDOPHYTIC FUNGUS FROM <i>Alibertia macrophylla</i> (Rubiaceae)

Gubiani, Juliana R.; Habeck, Thomas R.; Chapla, Vanessa M.; Silva, Geraldo H.; Bolzani, Vanderlan S.; Araujo, Angela R.

doi:10.21577/0100-4042.20160169

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Artigo • Quím. Nova 39 (10) • Dec 2016 • https://doi.org/10.21577/0100-4042.20160169 copy

ONE STRAIN-MANY COMPOUNDS (OSMAC) METHOD FOR PRODUCTION OF PHENOLIC COMPOUNDS USING Camarops sp., AN ENDOPHYTIC FUNGUS FROM Alibertia macrophylla (Rubiaceae)^# # This paper is part of the PubliSBQ Special Issue in honor of the late Prof Angelo da Cunha Pinto.

Authorship SCIMAGO INSTITUTIONS RANKINGS

Seven phenolic derivatives including p-hydroxyphenyllactic acid (1), p-hydroxybenzoic acid (2), p-hydroxybenzaldehyde (3), phenyllactic acid (4), n-butyl-3,4-dihydroxybenzoate (5), n-hexyl-3,4-dihydroxybenzoate (6) and n-octyl-3,4-dihydroxybenzoate (7) were produced using Camarops sp. via the one strain-many compounds (OSMAC) approach. Their structures were determined using 2D NMR and ESI-MS spectra and were compared with works reported in the literature. This paper deals with the first report of these compounds in Camarops sp.

Keywords:
endophytic fungus; Camarops sp.; phenolic compounds

Position	1		Position	2		Position	3		Position	4		Position	5
Position	δ ¹H	δ ¹³C	Position	δ ¹H	δ ¹³C	Position	δ ¹H	δ ¹³C	Position	δ ¹H	δ ¹³C	Position	δ ¹H	δ ¹³C
1	-	155.7	1	-	161.6	1	-	163.3	1	7.23 (m)	125.9	1	-	112.6
2	6.63 (d, 8.2)	114.4	2	6.81 (d, 8.7)	114.9	2	7.75 (d, 8.5)	132.0	2	7.23 (m)	127.8	2	7.17 (d, 2.0)	113.6
3	7.00 (d, 8.2)	129.8	3	7.76 (d, 8.7)	131.1	3	6.92 (d, 8.5)	115.8	3	7.23 (m)	129.3	3	-	149.6
4	-	130.4	4	-	121.9	4	-	129.3	4	-	138.3	4	-	153.0
5	7.00 (d, 8.2)	129.8	5	7.76 (d, 8.7)	131.1	5	6.92 (d, 8.5)	115.8	5	7.23 (m)	129.3	5	6.82 (d, 8.0)	117.7
6	6.63 (d, 8.2)	114.4	6	6.81 (d, 8.7)	114.9	6	7.75 (d, 8.5)	132.0	6	7.23 (m)	127.8	6	6.98 (dd, 2.0; 8.0)	123.4
7a	2.62 (m)	39.3	7	-	167.7	7	9.79 (s)	190.8	7	2.75 (dd; 10.0; 5.0) 2.96 (dd; 10.0; 5.0)	40.0	1’	-	168.8
7b	2.85 (dl, 12.8)	39.3							8	4.11 (dd; 5.0; 5.0)	71.1	2’	4.30 (t, 6.5)	64.8
8	3.96 (sl)	71.4							9	-	175.1	3’	1.72 (m)	27.2
9	-	175.5										4’	1.37 (m)	27.2
												5’	0.91 (t, 7.0)	13.4

Sociedade Brasileira de Química Instituto de Química, Universidade Estadual de Campinas (Unicamp), CP6154, 13083-0970 - Campinas - SP - Brazil
E-mail: quimicanova@sbq.org.br

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ONE STRAIN-MANY COMPOUNDS (OSMAC) METHOD FOR PRODUCTION OF PHENOLIC COMPOUNDS USING Camarops sp., AN ENDOPHYTIC FUNGUS FROM Alibertia macrophylla (Rubiaceae)# # This paper is part of the PubliSBQ Special Issue in honor of the late Prof Angelo da Cunha Pinto.

ONE STRAIN-MANY COMPOUNDS (OSMAC) METHOD FOR PRODUCTION OF PHENOLIC COMPOUNDS USING Camarops sp., AN ENDOPHYTIC FUNGUS FROM Alibertia macrophylla (Rubiaceae)^# # This paper is part of the PubliSBQ Special Issue in honor of the late Prof Angelo da Cunha Pinto.